3.3. SAFETY ASPECTSIn spray drying operations a potential danger of explosion and fire can exist under certain conditions [7].Fire hazards exist if any of the following conditions occur:. The temperature of the air-product mixturereaches a flammability limit (see Table 10.8).. The oxygen content in the drying medium ishigh.(See relevant chapter of this handbook for details onfire and explosion hazards.)Dry skim milk has the lowest inflammation temperature in a layer; sugar and some detergents havethe lowest temperature when in a cloud in a spraydryer. Temperature data for the drying medium in aspray dryer for three typical materials are shown inFigure 10.43. The temperatures are given at the following locations: T1, heater outlet; T2, drying chamber inlet; T3, drying chamber outlet; T4, exhaust air;T5, pneumatic transport location. Useful data for minimum ignition temperatures of milk products canbe found in Ref. [34].It is evident that the drying air temperature nearlyalways exceeds the inflammation temperature in athe layer. This means that ignition is possible wheneverdry powder deposits are well-formed. In the case of detergents, ignition is also possible in the cloud.Ignition may be initiated for any one of the following reasons:. Spontaneous combustion in product deposits. Hot solid particles entering the dryer withgas drying. Spark generation through friction. Electrical failure. Static electricity dischargeFire prevention methods are based on proper operation and cleaning of the dryer. An important safetydevice is an automatic control system (ACS), as it canmaintain the temperature within + 18 c range whereasthe manually controlled temperature may vary + 108C.The control system should include a detection systemof parameter, deviation detection, gas drying depositanalysis, and continuous monitoring of the humidityand temperature at selected locations.The explosion hazard depends on the value of thecritical particle concentration hand, oxidation velocity, andthe explosion pressure. If any one of these conditionsis reached, there is danger of ignition. A comparisonof both explosive and process concentration hand forthree products is shown in Figure 10.44. The powderconcentrations are given in the following locations:C1, drying chamber; C2, cyclones; C3, the exhaust fan;C4, wet scrubber; and C5, pneumatic transport. 10.44 the figure shows that even under normal operating conditions the danger of explosion does exist in anormal spray dryer. The explosion hazard is highabove the solid line. The zone between the thick anddotted lines is potentially dangerous as the powderconcentration hand there exceeds 50%. All processequipment in which the operating dust concentration handexceeds 50% of the lower explosive concentration handmust be provided with a safety device. The spraydrying chamber, cyclones, and pipes should beequipped with safety doors and explosion vents [19].When highly inflammable materials are dried it isnecessary to use inert atmosphere. A gastight closedcycle spray dryer with nitrogen as the drying mediummay be used in such cases. When explosion hazardexists, a self-inertizing system is recommended. Goodmaintenance practice cannot be overemphasized.For additional information and further referenceson fire and explosion hazards in drying of solids ', theReader is referred to the appropriate chapter in thisHandbook.
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