dry G4 Gooch crucible in a oven at 105. Wash the crucible with 10 ml of ethyl alcol, then with 10 ml of ethyl ther. dry for 30 minutes at 98 to 100, cool in a desiccator and weigh.to 1 g of sample, weighed accurately add 80 ml of 1: 1 volume of water: ethanol in a 100 ml. stir for 15 minutes vigourously. Add 0.4 ml of fehling solution (A), and 0.35 ml of the standard sodium hydroxide solution. graduated flask flask
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